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The crystal structure of the title compound, Ru 3 ( μ -Ph 2 AsCH 2 AsPh 2 )(CO) 10  has been determined at room temperature. Crystals are monoclinic,  P 2 1 / c ,  a  = 13.307(3),  b  = 11.972(2),  c  = 24.158(4) Å,  β  = 107.92(5)°,  Z  = 4,  D m   = 2.03,  D x   = 1.92 Mg m −3 . The structure was refined by a blocked full-matrix least-squares procedure to final  R  = 0.070 and  R w   = 0.077 for 5699 unique reflections used [ I  &gt; 2.5  σ ( I )] out of 6778. The structure shows that the Ph 2 AsCH 2 AsPh 2  group that bridges a Ru – Ru bond occupies equatorial positions. Interatomic distances of interest are Ru(1) – Ru(2) = 2.845(1), Ru(1) – Ru(3) = 2.817(1), and Ru(2) – Ru(3) = 2.840(1) Å.

The structure of l,2- μ -[bis(diphenylarsino)methane-As,As′]-1,1,1,2,2,2,3,3,3,3-decacarbonyl- triangulo -triruthenium(0)