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The pyrochlore-related structure (trigonal  P 3 1 21,  a  = 7.191 Å,  c  = 17.402 Å) proposed previously for Mn 2 Sb 2 O 7  on the basis of powder X-ray diffraction data has been confirmed and refined using neutron diffraction data. The atomic coordinates and bond lengths obtained are more precise than those reported previously: average bond lengths of 2.46 Å and 1.96 Å are consistent with Mn 2+  and Sb 5+  in 8- and 6-fold coordination respectively by O 2− . Data has been analysed by the two-stage profile decomposition method.

zeitschrift für kristallographie

Refinement of the crystal structure of the manganous antimonate Mn 2 Sb 2 O 7  with neutron powder diffraction data by the profile decomposition method