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The crystal structures of three benzanilide derivatives, which are oligomers of fire resistant polymers, are reported. The compound (I) is monoclinic,  P 2 1  c , with  a  = 12.430(2),  b  = 13.535(2),  c  = 7.948(2) Å,  β  = 108.18(3)°; compound (II) is orthorhombic,  P 2 1 2 1 2 1 , with  a  = 25.236(2),  b  = 9.019(2),  c  = 5.639(1) Å, compound (III) is monoclinic,  P 2 1 / a , with  a  = 23.622(3),  b  = 9.581(2),  c  = 10.373(2) Å,  β  = 99.08(3)°. The three structures have been solved by direct methods and refined to  R  = 0.042 for 1740, to  R  = 0.049 for 1200 and to  R  = 0.050 for 3811 observed reflections for compounds (I), (II) and (III) respectively.

Crystal structure of 2-carboxy-2′-methylbenzanilide, of 2-carboxy-3′-methylbenzanilide and of 2-carboxy-benzanilide 1