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The absolute configuration of the title compound which shows a pharmacologic activity was determined by the Bijvoet difference method. The compound crystallizes in the orthorhombic system, space group  P 2 1 2 1 2 1 , with  a  = 10.292(2) Å,  b  = 12.777(2) Å,  c  = 20.471(2) Å. The final values are  R  = 0.031 and  R w   = 0.032 for 2920 reflections. The results establish that the camphosulfonate, modulus A, has the  R  configuration and the methyl  α -(tetrahydro-4,5,6,7 thieno (3,2-c) pyridin-5-yl)-acetate, modulus B, exhibits the  S  configuration.

zeitschrift für kristallographie

Structure cristalline et moléculaire du camphosulfonate de l' α -(tétrahydro-4,5,6,7 thiéno (3,2-c) pyridyl-5) (chloro-2 phényl)-acétate de méthyle, C 26 H 32 NO 6 S 2 Cl. Configuration absolue