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[C(NH 2 ) 3 ] 2 (+)C 4 H 4 O 6  · H 2 O crystallizes in space group  P 2 1  with  a  1  = 4.760(2),  a  2  = 14.151(4),  a  3  = 9.852(3) Å,  α  2  = 102.97(3)°,  Z  = 2,  D c   = 1.472,  D m   = 1.469 g cm −3 . The structure was solved by direct methods employing 3752 independent X-ray reflections (Mo Kα ). The refinement converged at  R  = 0.043 ( R w   = 0.032). The guanidinium ions and also the tartrate ions show quite normal geometrical details as observed in similar compounds. The ions are linked by hydrogen bonds.

Crystal structure and physical properties of monoclinic guanidinium tartrate hydrate, [C(NH 2 ) 3 ] 2 (+)C 4 H 4 O 6 · H 2 O*