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The crystal structure of the title compound (DPXI hereafter) was determined from three-dimensional intensities of 2397 independent reflections. The cell constants obtained from direct  θ  value measurements of 100 reflections and refined by least-squares, are  a  = 10.637(1),  b  = 10.440(2),  c  = 7.844(1) Å,  α  = 82.53(2)°,  β  = 107.75(1)°,  γ  = 102.42(1)°,  Z  = 2, space group  P [unk],  ϱ  meas  = 1.69 Mg m −3 .

The crystal structure of (diphenyl) (ethylxanthogenate)iodane, C 15 H 15 IOS 2