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Mr = 460.36, monoclinic.  P 2 1 / c ,  a  = 13.718(1),  b  = 11.090(1),  c  = 14.985(1) Å,  β  = 98.162(2)°,  V  = 2256.67(9) Å 3 ,  Z  = 4,  D x   = 1.355 Mgm −3 ,  μ  = 0.933 mm −1 ,  F (000) = 968, room temperature, final  R  = 0.047 ( R w   = 0.048) for 3184 [ I  ⩾ 3  σ ( I )] observed reflections. The title compound has the “three-legged piano stool” geometry, i.e. the coordination geometry of the iron can be regarded as a distorted octahedron with a η  5  – C 5 Me 5  group occupying three coordination sites. Like its nonmethylated analogue it contains an unusually monodentate dithiophosphate ester ligand.

Crystal structure of ( η 5 -pentamethylcyclopentadienyl) (O,O′-diisopropyldithiophosphato) (dicarbonyl)-iron(II), FeS 2 PO 4 C 18 H 29