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In a PbO/PbF 2  flux (1400°C) a new (Al,Ge)-mullite was grown incorporating Pb 2+  and Nd 3+  ions, the needle like crystals (about 2 mm in length) are orthorhombic:  P 2 1 2 1 2,  a  = 7.6648(4),  b  = 7.7914(3),  c  = 2.9213(1) Å,  V  = 174.46(1) Å 3 ,  Z  = 1,  D  x  = 3.79 g cm −3 . Final  R  = 0.0211 for 297 observed reflections. Pb 2+  and Nd 3+  are located in the vacancies that are formed by omission of O(3)-atoms.

A Pb/Nd-stabilized mullite of the composition Al 5.03 Ge 0.97 Pb 0.15 Nd 0.06 O 9.71