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The crystal structure of Gysinite has been determined at the composition La 0.16 Nd 1.18 Pb 0.66 (CO 3 ) 2 (OH) 1.34  · 0.66 H 2 O, M r  = 483.85. Orthorhombic space group  Pmcn ,  a  = 5.0028(8),  b  = 8.555(1) and  c  = 7.2392(8) Å,  V  = 309.83 Å 3 ,  Z  = 2,  D x   = 5.18 g · cm −3 . Single crystal X-ray refinement, Mo Kα ,  λ  = 0.7107 Å,  μ  = 34.8 mm −1 ,  F (000) = 425.4, room temperature,  R  = 0.065 for 368 independent contributing reflections. The Pb-containing Gysinite is isostructural to the Ca and Sr analog Ancylite and to synthetic hydroxy-carbonates of lanthanides elements.

Structure refinement of Gysinite La 0.16 Nd 1.18 Pb 0.66 (CO 3 ) 2 (OH) 1.34 · 0.66 H 2 O