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Synthetic dodecasil 3C, 136 SiO 2  · 16 M 12  · 8 M 16 , is cubic with space group  Fd 3 and  a  0  = 19.402(1) Å. Structure refinement of a crystal containing M 12  = N 2  and small amounts of CH 4  and Ar, M 16  = N(CH 3 ) 3  and CO 2  led to a weighted  R w   = 0.064 for 883 independent reflexions. The clathrate compound is isotypic with the cubic clathrate hydrate type II.

Studies on Clathrasils. VI*: Crystal structure of dodecasil 3C, another synthetic clathrate compound of silica