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Lead tetrasodium trimetaphosphate PbNa 4 (P 3 O 9 ) 2  is triclinic,  P [unk] with  a  = 7.268(4),  b  = 8.151(5),  c  = 7.851(5) Å,  α  = 121.52(5),  β  = 102.06(5),  γ  = 73.00(5)°,  Z  = 1,  V  = 378.3 Å 3  and  d x   = 3.393 g/cm 3 . Its crystal structure has been solved using 1507 reflexions, with a final  R  value 0.049 for 1268 reflexions. The atomic arrangement is characterized by a disorder between Pb and Na on one crystallographic site. Chemical preparation and crystal data are given for the isotypic barium salt: BaNa 4 (P 3 O 9 ) 2 .

Crystal structure of lead-tetrasodium trimetaphosphate: PbNa 4 (P 3 O 9 ) 2 , Crystal data for BaNa 4 (P 3 O 9 ) 2