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Solid solutions of Mn(II), Fe(II), or Mg in nickel-hexahydroxoheptaoxo-hexaborate-ethanol-3.5 water, Ni x M 1 – x [B 6 O 7 (OH) 6 ] · C 2 H 5 OH · 3.5 H 2 O ( M  = Mn: x  = 0.8, 0.75, or 0.67;  M  = Fe: x  = 0.75;  M  = Mg:  x  = 0.75), have been crystallized. The crystal structure of one of these compounds with Mn(II), Ni 0.8 Mn 0.2 (H 2 O) 3 [B 6 O 7 (OH) 6 ] · C 2 H 5 OH · 0,42 H 2 O, has been determined from single-crystal X-ray diffractometer data. The compound crystallizes in the monoclinic space group P2 1 /c. The lattice constants are  a  = 9.586(1) Å, b  = 12.420(3) Å, and  c  = 14.645(3) Å;  β  = 106.62(5)°; V = 1673.01 Å 3 ; the unit cell contains four formula units; the measured density was  D m   = 1.74 and the calculated density was  D c   = 1.76 g · cm −3 .

Die Kristallstruktur von Ni 0.8 Mn 0.2 (H 2 O) 3 [B 6 O 7 (OH) 6 ] · C 2 H 5 OH · 0.42 H 2 O; feste Lösungen von Metall(II)-Ionen in Nickelhexaborat