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The bicyclic phosphorus compound 2,3,4,6-Tetra- tert -butylbicyclo[3.1.0]hexaphosphane  t -Bu 4 P 6 , C 16 H 36 P 6  crystallizes in the monoclinic space group  P 2 1 / n  with  a  = 912.0 pm,  b  = 1383.8 pm,  c  = 1951.4 pm,  β  = 90.93° and  Z  = 4 formula units. The crystal structure has been worked out by single crystal X-ray methods and refined to  R  = 0.045 with 860 observed reflections.

zeitschrift für kristallographie

Beiträge zur Strukturchemie phosphorhaltiger Ketten und Ringe: VI. Die Molekül- und Kristallstruktur des 2,3,4,6-Tetra- tert -butylbicyclo[3.1.0]hexaphosphans,  t -Bu 4 P 6 *