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Single crystals of Pb 2 [UO 2 ][TeO 3 ] 3  were obtained by hydrothermal synthesis. The crystal data are:  a  = 11.605(4),  b  = 13.389(17),  c  = 6.981(l)Å,  β  = 91.23(3)°,  Z  = 4,  D  x  = 7.42(1)g·cm −3 . The structure was determined from X-ray intensities measured on a two-circle diffractometer and was refined for 2566 independent observed reflections to  R  = 0.059. It can be described as built up by {[UO 2 ][TeO 3 ] 3 } n  4n−  sheets parallel to (010) which are connected by lead atoms in irregular coordination.

Synthesis and crystal structure determination, of Pb 2 [UO 2 ][TeO 3 ] 3