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The structure of the title compound, C 11 H 38 B 18 CoNO was solved using X-ray diffraction techniques. The crystals are orthorhombic, space group  Pna 2 1  with  a  = 12.508(7),  b  = 15.935(2), c  = 12.618(2) Å,  Z  = 4. The structure has been determined by the heavy-atom method and refined by the full-matrix least-squares method up to  R  = 0.066 for 1621 counter reflections. The ionic structure consists of the [N(C 2 H 5 ) 3 CH 3 ] +  cation and the [O(C 2 B 9 H 10 ) 2 Co] −  anion. The anion is built from two dicarbollide ligands sharing the cobalt atom as a common apex. Moreover, these two ligands are linked by a monoatomic oxygen bridge. The pentagonal planes bound to the cobalt atom are not parallel in the anion, but inclined to each other by an angle of 28.3°, which is caused by the oxygen bridge.

zeitschrift für kristallographie - crystalline materials

The crystal and molecular structure of Methyltriethylammonium  μ -8,8′-oxa-3,3′- commo -bis(undecahydro-1,2-dicarba-3-cobalta- closo -dodecaborate) (1-), [N(C 2 H 5 ) 3 CH 3 ] + · [O(C 2 B 9 H 10 ) 2 Co] −