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The crystal structure of the garnet {Mn 3 }[Fe 2 ](Ge 3 )O 12  has been refined by least-squares calculations applied to single-crystal data collected with a Buerger-Supper-Pace-Picker automatic diffractometer. The Ge–O distance is 1.77 ± 0.02 Å (limits of error), about 0.03 Å longer than the Ge–O distance in quartz-type GeO 2 . This is in accord with the analogous Si–O distances. The Fe–O distance is 2.00 ± 0.02 Å in good agreement with the analogous distance in three iron garnets. The Mn–O distances are 2.30 and 2.42 ± 0.02 Å. The structural results are in accord with the absence of ferrimagnetism in the {Mn 3 }[Fe 2 ](Ge 3 )O 12  garnet.

Crystal structure of the garnet {Mn 3 }[Fe 2 ](Ge 3 )O 12