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The aim of this study was to investigate the use of electrophilic radioiodination in the labelling of  closo -monocarborane(-1). Ammonio- closo -monocarborane (ACMC, 1NH 3 1CB 11 H 11 ) was labelled with  125 I using Chloramine-T as an oxidant. Radio-TLC was used for analysis. Influence of substrate amount, oxidant concentration, and pH of the reaction media on the labelling yield was studied. A labelling yield of 80%-90% was obtained. The results of the study indicate feasibility to use derivatives of  closo -monocarborane(-1) as a pendant group for indirect radioiodination of proteins, and for studying pharmacokinetics of boron-rich compounds for BNCT.

Radioiodination of ammonio- closo -monocarborane, 1-H 3 N-1-CB 11 H 11 . Aspects of labelling chemistry in aqueous solution using Chloramine-T