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The PET radionuclide  76 Br (t 1/2 =16.2 h) can be easily produced utilizing the nuclear reaction As( 3 He,2n) 76 Br. We use high-purity arsenic targets and isolate radioactive bromide by chromic acid oxidation followed by simple distillation of [ 76 Br] hydrogen bromide using a semi-remote apparatus. Use of reagents with little or no carrier bromine yields high specific activity radiobrominated pharmaceuticals prepared from the distilled [ 76 Br] hydrogen bromide.

Semi-remote production of Br-76 and preparation of high specific activity radiobrominated pharmaceuticals for PET studies