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The effect of subtle variations on zirconium molybdate- 99 Mo gel preparatory conditions, such as stoichiometry of reactants, pH of gel formation, conditioning of gel granules  etc.  , prior to elution were investigated primarily to arrive at the conditions resulting in high  99m Tc release and minimal  99 Mo breakthrough upon elution with normal saline. Zirconium molybdate-  99 Mo gels were prepared by reacting solutions of Zr and Mo in mole ratios of 0.75-1.5. Both water and normal saline were used for gel disintegration, and the release of  99m Tc and  99 Mo from gel columns into eluates was compared. Sharper elution profile of  99m Tc, but with significantly higher  99 Mo breakthrough (5-8 times), was obtained when water alone was used for disintegration and elution, in comparison to when saline was used.

radiochimica acta

99m Tc gel generators based on zirconium molybdate- 99 Mo: III: Influence of preparatory conditions of zirconium molybdate- 99 Mo gel on generator performance