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A new polyoxometalate of chemical formula, Na 2 (H 2 O) 4 (H 3 O)[Al(OH) 6 Mo 6 O 18 ] (1) containing Anderson type large anion has been synthesized and characterized by single-crystal X-ray structure determination and IR spectroscopic studies. The crystal of 1 is triclinic, spacegroup P−1 with cell dimensions,  a  = 6.365(9)Å,  b  = 10.37(1)Å,  c  = 10.44(1)Å and α = 65.41(1), β = 77.18(1), γ = 86.58(1) and  Z  = 1. The compound 1 behaves as an ion exchanger and is stable in thermal, radiation and chemical environments. Radiochemical separation of the short-lived daughter  137m Ba ( t  1/2  = 2.50 min) from its long-lived parent  137 Cs using this newly designed and synthesized ion exchanger has been developed.

Separation of 137m Ba from 137 Cs using new ion exchanger Na 2 (H 2 O) 4 (H 3 O)[Al(OH) 6 Mo 6 O 18 ]