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H18NaO12PSSr, cubic, P213 (no. 198), a = 10.917(1) Å, V = 1301.1 Å, Z = 4, Rgt(F) = 0.041, wRref(F) = 0.087, T = 223 K. Source of material Trisodium monothiophosphate, Na3[PO3S], was synthesized from aqueous solutions of NaOH and PSCl3 according to [1]. A solution of sodium strontium monothiophosphate nonahydrate was obtained by adding SrCl2 · 6H2O (1.50 g, 5.626 mmol) to a solution of Na3[PO3S] (1.01 g, 5.626 mmol) in 40 mL distilled water at 40 °C. Slowly cooling at room temperature yielded cubeshaped colorless crystals of the title compoundwithin somedays. Experimental details The H atom parameters were refined freely except those which did not converge. The latter ones were fixed, positional parameters at the parameters found from Fourier difference maps and Uiso at 0.05 Å.

Crystal structure of sodium strontium monothiophosphate nonahydrate, NaSr[PO 3 S] · 9H 2 O