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C 20 H 14 O 4 , monoclinic,  P 12 1 / c 1 (no. 14),  a  = 12.5632(6) Å,  b  = 4.3769(2) Å,  c  = 14.8059(8) Å, β = 104.213(2)°,  V  = 789.2 Å 3 ,  Z  = 2,  R  gt  (F)  = 0.053,  wR  ref  (F  2  )  = 0.145,  T  = 200 K.

Crystal structure of 2-[6-(2-formylphenoxy)-2,4-hexadiynyloxy]- benzaldehyde, C 20 H 14 O 4