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C 37 H 34 Br 2 O 7 , triclinic,  P 1 (no. 2),  a  = 9.744(1) Å,  b  = 10.059(1) Å,  c  = 18.012(2) Å, α = 91.66(1)°, β = 99.06(1)°, γ = 104.536(9)°,  V  = 1683.4 Å 3 ,  Z  = 2,  R  gt  (F)  = 0.071,  wR  ref  (F  2  )  = 0.180,  T  = 293 K.

Crystal structure of 5,17-dibromo-25,27-dimethoxy-26-benzoyloxy- 28-hydroxycalix[4]arene dihydrate, C 37 H 34 Br 2 O 5 · 2H 2 O