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C 8 H 10 N 2 O 6 S 2 , monoclinic,  P 12 1 / n 1 (No. 14),  a  = 7.6806(5) Å,  b  = 12.8546(8) Å,  c  = 12.2389(7) Å, β = 97.071(2)°,  V  = 1199.2 Å 3 ,  Z  = 4,  R  gt  (F)  = 0.035,  wR  ref  (F  2  )  = 0.099,  T  = 273 K.

Crystal structure of the adduct of sulfosalicylic acid and thiourea, C 7 H 6 O 6 S · CH 4 N 2 S