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C 10 H 9 MoN 3 O 4 , monoclinic,  C 12/ c 1 (No. 15),  a  = 12.904(2) Å,  b  = 12.771(2) Å,  c  = 9.211(1) Å, β = 116.16(2)°,  V  = 1362.5 Å 3 ,  Z  = 4,  R  gt  (F)  = 0.064,  wR  ref  (F  2  )  = 0.156,  T  = 193 K.

Crystal structure of bisacetonitrile-tetracarbonylmolybdenum— acetonitrile solvate, Mo(CO) 4 (NCCH 3 ) 2 · CH 3 CN