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C 24 H 8 O 6 , monoclinic,  P 12 1 / n 1 (No. 14),  a  = 3.703(6) Å,  b  = 12.013(5) Å,  c  = 17.161(3) Å, β = 93.26(6)°,  V  = 762.2 Å 3 ,  Z  = 2,  R  gt  (F)  = 0.045,  wR  ref  (F  2  )  = 0.128,  T  = 223 K.

Refinement of the crystal structure of α-3,4:9,10-perylenetetracarboxylic dianhydride, C 24 H 8 O 6 , at 223 K