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Li 1.5 Al 0.5 Ti 1.5 (PO 4 ) 3  (LATP) powders were prepared from different NO   x   -free precursors using an aqueous-based solution-assisted solid-state reaction (SA-SSR). The sintering behavior, phase formation, microstructure and ionic conductivity of the powders were explored as a function of sintering temperature. The powders showed a relatively narrow temperature windows in which shrinkage occurred. Relative densities of 95% were reached upon heating between 900 and 960 °C. Depending on the morphological features of the primary particles, either homogeneous and intact microstructures with fine grains of about &lt;2 µm in size or a broad grain size distribution, micro-cracks and grain cleavages were obtained, indicating the instability of the microstructure. Consequently, the ceramics with a homogeneous microstructure possessed a maximum total ionic conductivity of 0.67 mS cm −1 , whereas other ceramics reached only 0.58 mS cm −1  and 0.21 mS cm −1 .

Sintering behavior and ionic conductivity of Li 1.5 Al 0.5 Ti 1.5 (PO 4 ) 3 synthesized with different precursors