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α-Alkoxyalkyl radicals with a leaving group L = Cl or OCOCH 3  in β-position are produced by H-abstraction from the corresponding saturated substrates by  · OH, SO ·  4  -  or (CH 3 ) 3 CO ·  radicals. From ESR spectroscopic observations it is concluded that in aqueous solution at pH 5 -9 the following fast hydrolysis reactions take place:

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Model Reactions for the Degradation of DNA-4′ Radicals in Aqueous Solution. Fast Hydrolysis of α-Alkoxyalkyl Radicals with a Leaving Group in β-Position Followed by Radical Rearrangement and Elimination Reactions