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Direct alkylation via a free radical reaction was utilized to prepare 8-tert-butylguanosine-5′- phosphate; this was dephosphorylated with alkaline phosphatase to give the parent nucleoside. The 8- (α-hydroxyisopropyl) derivatives of 5′-GMP and guanosine were prepared in an analogous manner.

zeitschrift für naturforschung c

Purine Nucleosides and Nucleotides Unequivocally in the Syn Conformation: Guanosine and 5′-GM P with 8-tert-Butyl and 8-( α-Hydroxyisopropyl) Substituents