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The non methylene interrupted cis,cis-octadecadienoic acids from human milk fat were pre­pared by thin layer chromatography on AgNO 3  impregnated silicagel plates. The position of double bonds was determined by hydroxylation of the double bonds with OsO 4  followed by silylation. The corresponding O-trimethylsilylether derivatives of the fatty acid methyl esters were analyzed by gaschromatography mass spectrometry. 14 isomers of the following series could be identified: C 18:2  ⊿9. (12.13.14.15.16.17) ; C 18:2  ⊿ (6.7.8.9.).12; C 18:2  ⊿ (10.11.12.).15 (⊿18.15) ; C 18:2  ⊿5.9-, ⊿6.10; ⊿10.14; (⊿12.16). Possible biosynthetic pathways are discussed.

zeitschrift für naturforschung c

Nicht methylenunterbrochene cis,cis-Octadecadiensäuren Minor Constituents of Human Milk, VI Non Methylene Interrupted cis,cis-Octadecadienoic Acids: Inhaltstoffe der Frauenmilch, VI