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The praseodymium metaborate molybdate(VI) PrBO 2 MoO 4  was synthesized by solid-state reaction methods at 850 °C under an argon atmosphere and identified by its powder X-ray diffraction pattern. The polycrystalline sample was placed in a Walker-type multianvil press, where pressure-induced crystal growth at 1 GPa and 850 °C was successful, yielding single crystals suitable for structure determination. PrBO 2 MoO 4  crystallizes monoclinically in the space group  P 2 1 / c  (no. 14) with the unit cell parameters  a  = 10.1735(2),  b  = 4.1479(1),  c  = 11.9090(3) Å,  β  = 116.52(1)°, and four formula units per cell.

On the synthesis and crystal structure of praseodymium(III) metaborate molybdate(VI) – PrBO 2 MoO 4