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By utilizing the well-known selective xanthine oxidase inhibitor topiroxostat, a new zinc(II) complex Zn(L) 2 (H 2 O) 2  ( 1 ) [HL = 4-(3-(pyridine-4-yl)-1 H -1,2,4-triazol-5-yl)picolinic acid] has been hydrothermally synthesized, involving  in-situ  ligand formation upon hydrolysis of topiroxostat. The complex has been structurally characterized by elemental analysis, IR spectroscopy, thermogravimetric analysis, powder X-ray diffraction, and single-crystal X-ray diffraction. X-ray structural analysis revealed that complex  1  is a N,O-chelating mononuclear Zn(II) complex. Complex  1  shows good thermal stability and exhibits photoluminescence in the solid state at room temperature. Moreover, complex  1  has been shown to be effective in the solvent-free ring-opening polymerization of  ε -caprolactone without any co-catalyst or initiator.

zeitschrift für naturforschung b

Synthesis, characterization, luminescence, and catalytic properties of a zinc(II) complex with a N,O-donor ligand generated  in situ  from topiroxostat