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The autoreduction of ammonium pertechnetate in solutions of trifluoromethanesulfonic acid (triflic acid, TfOH) and trifluoromethanesulfonic anhydride (triflic anhydride, TfOTf) results, in the presence of sodium ions, in the formation of the complex Na 2 [(Tc V O)(OTf) 5 ] · 2(TfOH). Its structure has been determined by single-crystal X-ray diffraction.

Crystal structure of the oxidotechnetate(V) complex Na 2 [(Tc V O)(OTf) 5 ] · 2(TfOH) with TfOH = trifluoromethanesulfonic acid