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Phase analytical studies in the scandium-rich parts of the Sc- T -In systems ( T  = Fe, Au) revealed the formation of small areas of solid solutions Sc 2− x   Fe   x   In and Sc 2 Au   x   In 1− x    that are derived from the binary Ni 2 In-type phase Sc 2 In, space group  P 6 3 / mmc . The samples were synthesized from the elements in sealed tantalum ampoules in an induction furnace. The structures of Sc 1.88 Fe 0.12 In ( a  = 498.37(6),  c  = 630.94(8) pm, w R 2 = 0.0603, 124  F   2  values, nine variables), Sc 2 Au 0.37 In 0.63  ( a  = 494.65(5),  c  = 632.42(6) pm, w R 2 = 0.0639, 123  F   2  values, nine variables) and Sc 2 Au 0.22 In 0.78  ( a  = 496.09(3),  c  = 628.29(4) pm, w R 2 = 0.0331, 124  F   2  values, nine variables) were refined from single-crystal diffractometer data. Sc 1.88 Fe 0.12 In shows Sc/Fe mixing on Wyckoff position 2 a , while gold is substituted for indium on site 2 c . Analyses of the reciprocal space gave no hint for superstructure formation, and the three refinements show slightly enhanced  U   33  displacement parameters for the 2 d  scandium sites which react on the mixed occupancies.

Sc 2 In-based solid solutions in the Sc-Fe-In and Sc-Au-In systems