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Several Lu 26   T   17− x   In   x    ( T  = Rh, Ir, Pt) phases with varying  x  values were obtained by induction-melting reactions of the elements in sealed tantalum ampoules. All samples were characterized through their X-ray powder diffraction patterns. These compounds crystallize with the tetragonal Sm 26 Co 11 Ga 6 -type structure, space group  P 4/ mbm  and  Z  = 2. The structure of Lu 26 Pt 7.55 In 9.45  has been refined from single-crystal X-ray diffractometer data:  a  = 1165.32(5),  c  = 1547.46(6) pm, w R 2 = 0.0895, 2173  F   2  values and 70 variables. The Lu 26   T   17− x   In   x    phases are the first indium representatives of the Sm 26 Co 11 Ga 6  type. They belong to the  n  = 4 members of Parthé’s  A   5 n +6   B   3 n +5  series, which show different stacking sequences of square prisms and antiprisms. Lu 26 Pt 7.55 In 9.45  as a lutetium-rich intermetallic compound exhibits a broader range of shorter Lu–Lu distances (341–375 pm). Temperature dependent magnetic susceptibility measurements show Pauli paramagnetism for Lu 26 Ir 8.5 In 8.5  and Lu 26 Rh 7 In 10  with room temperature values of the magnetic susceptibility of  χ  = 1.53 × 10 −3  emu mol −1  for Lu 26 Rh 7 In 10  and  χ  = 6.54 × 10 −4  emu mol −1  for Lu 26 Ir 8.5 In 8.5 .

Lu 26 T 17– x In x ( T = Rh, Ir, Pt) – first indium intermetallics with Sm 26 Co 11 Ga 6 -type structure