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The ternary intermetallic phases  RE Pd 2 Zn 3  ( RE  = Y, La–Nd, Sm, Gd–Dy) were synthesized from the elements by induction melting in sealed niobium ampoules followed by annealing. The CaCu 5 -type samples (space group  P 6/ mmm ) were characterized through Guinier powder patterns. The structures of YPd 2 Zn 3  ( a  = 523.91(4),  c  = 430.88(3) pm,  wR 2 = 0.0570, 96  F  2  values, 9 variables) and NdPd 2 Zn 3  ( a  = 535.08(7),  c  = 427.81(6) pm,  wR 2 = 0.0217, 123  F  2  values, 9 variables) were refined from single-crystal X-ray diffractometer data. The zinc atoms form Kagome layers in AA stacking which leave trigonal prismatic voids for the palladium and hexagonal prismatic voids for the rare earth atoms. The Zn–Zn distances within the Kagome network of YPd 2 Zn 3  are 262 pm and the Pd–Zn distances in the Pd@Zn 6  trigonal prisms are 263 pm.

Ordered CaCu 5 -type phases RE Pd 2 Zn 3 ( RE = Y, La–Nd, Sm, Gd–Dy)