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The intermetallic scandium compounds Sc 1.024 Ir 2 In 0.976  and Sc 3 Ir 1.467 In 4  were synthesized by reactions of the elements in sealed tantalum ampoules at high temperature followed by annealing for crystal growth. Both structures were refined from single-crystal X-ray diffractometer data: MnCu 2 Al type,F  m   3  ‾   m    $Fm&amp;#x203e;{3}m$,  a  = 639.97(19) pm,  wR 2 = 0.0376, 41  F  2  values, seven variables for Sc 1.024 Ir 2 In 0.976  andP   6  ‾$P&amp;#x203e;{6}$,  a  = 769.99(5),  c  = 684.71(4) pm,  wR 2 = 0.0371, 967  F  2  values, 33 variables for Sc 3 Ir 1.467 In 4 . Sc 1.024 Ir 2 In 0.976  is a new Heusler phase with a small homogeneity range due to Sc/In and In/Sc mixing. The structure of Sc 3 Ir 1.467 In 4  is closely related to that of Sc 3 Rh 1.594 In 4  and belongs to the large family of ZrNiAl superstructures. The striking structural motif is the ordered stacking of empty In 6  and filled Ir@In 6  prisms with Ir–In distances of 269 pm.

Intermetallic phases in the Sc–Ir–In system – synthesis and structure of Sc 1.024 Ir 2 In 0.976 and Sc 3 Ir 1.467 In 4