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The  λ  6 Si-silicate [Cs(18-crown-6)] 2 [Si(OSO 2 CH 3 ) 6 ] ( 1 ) was synthesized by treatment of Si 2 Cl 6  with Cs[OSO 2 CH 3 ] in the presence of 18-crown-6. Compound  1  is the first example of a  λ  6 Si-silicate with a methanesulfonate ligand. It was characterized by NMR spectroscopy and by single-crystal X-ray diffraction. The solid-state structure of  1  consists of discrete [Si(OSO 2 CH 3 ) 6 ] 2–  anions and two [Cs(18-crown-6)] +  cations (triclinic space group,P   1  ¯    $P\overline{1}$,  Z  = 1).

Synthesis and structure of the λ 6 Si-silicate [Cs(18-crown-6)] 2 [Si(OSO 2 CH 3 ) 6 ]