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The rare earth oxoborates  RE B 5 O 8 (OH) 2  ( RE  = Ho, Er, Tm) were synthesized in a Walker-type multianvil apparatus at a pressure of 2.5 GPa and a temperature of 673 K. Single-crystal X-ray diffraction data provided the basis for the structure solution and refinement. The compounds crystallize in the monoclinic space group  C 2 (no. 5) and are composed of a layer-like structure containing  dreier  and  sechser  rings of corner sharing [BO 4 ] 5−  tetrahedra. The rare earth metal cations are coordinated between two adjacent  sechser  rings. Further characterization was performed utilizing IR spectroscopy.

High-pressure synthesis of RE B 5 O 8 (OH) 2 ( RE = Ho, Er, Tm)