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Single crystals of La 5 Ir 1.73 In 4.27  were grown from a sample of the starting composition 47La: 17Ir: 36 In by arc-melting, followed by a long annealing sequence in a muffle furnace. La 5 Ir 1.73 In 4.27  crystallizes with the Lu 5 Ni 2 In 4 -type structure, space group  Pbam , which was refined from single-crystal X-ray diffractometer data:  a  = 834.0(2),  b  = 1862.2(4),  c  = 385.31(8) pm,  wR 2 = 0.0278, 1165  F  2  values and 37 variables. The 4 h  iridium site shows a small degree of Ir/In mixing. Geometrically one can describe the La 5 Ir 1.73 In 4.27  structure as a simple 4:1 intergrowth variant of CsCl and AlB 2 -related slabs. The iridium and indium atoms form a one-dimensional meandering [Ir 1.73 In 4.27 ]  δ –  polyanion (292 pm Ir–In and 327 pm In–In) which is embedded in a lanthanum matrix.

La 5 Ir 1.73 In 4.27 with Lu 5 Ni 2 In 4 -type structure