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Microwave-assisted hydrothermal reaction of 2-fluoro-3,5,6-tri(1 H -1,2,4-triazol-1-yl)-1,4-benzenedicarbonitrile (L 1 ) with silver(I) nitrate yields a coordination polymer [Ag 3 (L 2 ) 2 (NO 3 )]  n   (1), in which the L 2  ligand (HL 2  = 2-hydroxy-3,5,6-tri(1 H -1,2,4-triazol-1-yl)terephthalonitrile) is obtained by in situ ligand transformation from the L 1  precursor. HL 2  monohydrate has also been isolated by the microwave-mediated hydrolysis of L 1  and structurally characterized. Single-crystal X-ray diffraction reveals that HL 2  monohydrate comprises a zwitterionic HL 2  moiety, while complex  1  displays an infinite L 2 -bridged double-chain structure. Given that the HL 2  molecule has a large conjugated  π  system, complex  1  exhibits strong blue luminescence in the solid state at room temperature.

Microwave synthesis of a blue luminescent silver(I) coordination polymer with a rigid tris-triazole ligand