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A new metal-organic framework, [Pb(hmpcaH) 2 ]  n   ( 1 ), has been hydrothermally synthesized from Pb(OAc) 2  · 3H 2 O and 2-hydroxy-6-methylpyridine-4-carboxylic acid (hmpcaH 2 ;  2 ), and characterized by IR spectroscopy, elemental and thermogravimetric analysis, and single-crystal X-ray diffraction. In complex  1 , each hmpcaH −  ligand represents a three-connected node to combine with the hexacoordinated Pb(II) ions, generating a 3D binodal (3,6)-connected  ant  network. The crystal structure of  2  was determined. The solid-state fluorescence properties of  1  and  2  were investigated.

A MOF based on a lead(II) 2-oxido-6-methylpyridine-4-carboxylate network