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The salt [NHEt 3 ][Re(I)(quinaldate)(CO) 3 Cl] was obtained by the reaction of Re(CO) 5 Cl with quinaldic acid and triethylamine in toluene. The crystal structure analysis of this salt revealed the presence of the complex anion [Re(quinaldate)(CO) 3 Cl] − , with the  d  6  Re(I) metal center in a pseudo-octahedral environment. The electronic spectra in absorption and emission exhibit bands which are attributed to quinaldate IL and CT transitions at comparable energies. The longest-wavelength emission originates from a Re(I) to quinaldate MLCT triplet, which can be quenched in solution by oxygen or triethylamine.

Synthesis, crystal structure and photoluminescence of [NHEt 3 ][Re(I)(quinaldate)(CO) 3 Cl]