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A novel three-dimensional Cd(II) coordination framework, [Cd(PTA)(BTBP) 0.5  · H 2 O]  n   ( 1 ) (BTBP =  4,4′-bis(1,2,4-triazol-1-ylmethyl)biphenyl; H 2 PTA =  p -phthalic acid), has been prepared and characterized through IR spectroscopy, elemental and thermal analysis, and single-crystal X-ray diffraction. The complex is a 5-connected network with the {4 5  · 6 6 } topology based on Cd- μ  2 -H 2 O-Cd chains. It exhibits strong fluorescent emission in the solid state at room temperature. Moreover, complex  1  shows high photocatalytic activity in the degradation of methylene blue under UV irradiation.

Photoluminescence and photocatalytic activity of a 3D framework based on 4,4′-bis(1,2,4-triazol-1-ylmethyl)biphenyl as a ligand for cadmium