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The synthesis and structural characterization of the new olefinic complex [Rh( η  5 -C 5 H 5 )(coe)(P t Bu 2 H)] ( 2 , coe =  cis -cyclooctene) is reported. The title compound was easily prepared in good yield by a thermolytic approach using [Rh( η  5 -C 5 H 5 )(coe) 2 ] ( 1 ) and the secondary phosphane in toluene under reflux conditions. The compound  2  has been characterized by NMR spectroscopy and microanalysis. Single crystals of  2  were grown from  n -hexane and the molecular structure has been established by X-ray diffraction.

Synthesis and molecular structure of [Rh( η 5 -C 5 H 5 )(coe)(P t Bu 2 H)] (coe= cis -cyclooctene)