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A potassium tetranitratopalladate(II) with the composition K 2 [Pd(NO 3 ) 4 ] · 2HNO 3  was synthesized by a simple solvothermal process in a glass ampoule. The new compound crystallizes in the monoclinic space group  P 2 1  /c  (no. 14) with the lattice parameters  a  = 1017.15(4),  b  = 892.94(3),  c  = 880.55(3) Å, and  β  = 98.13(1)° ( Z  = 2). The crystal structure of K 2 [Pd(NO 3 ) 4 ] · 2HNO 3  reveals isolated complex [Pd(NO 3 ) 4 ] 2−  anions, which are surrounded by eight potassium cations and four HNO 3  molecules. The complex anions and the cations are associated in layers which are separated by HNO 3  molecules. K 2 [Pd(NO 3 ) 4 ] · 2HNO 3  can thus be regarded as a HNO 3  intercalation variant of  β -K 2 [Pd(NO 3 ) 4 ]. The characterization is based on single-crystal X-ray and powder X-ray diffraction.

Serendipitous formation and characterization of K 2 [Pd(NO 3 ) 4 ]·2HNO 3