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The mixed cation triel borate Ga 4 In 4 B 15 O 33 (OH) 3  was synthesized in a Walker-type multianvil apparatus at high-pressure/high-temperature conditions of 12.5 GPa and 1300°C. Although the product could not be reproduced in further experiments, its crystal structure could be reliably determined  via  single-crystal X-ray diffraction data. Ga 4 In 4 B 15 O 33 (OH) 3  crystallizes in the tetragonal space group  I 4 1 / a  (origin choice 2) with the lattice parameters  a  = 11.382(2),  c  = 15.244(2) Å, and  V  = 1974.9(4) Å 3 . The structure of the quaternary triel borate consists of a complex network of BO 4  tetrahedra, edge-sharing InO 6  octahedra in dinuclear units, and very dense edge-sharing GaO 6  octahedra in tetranuclear units.

High-pressure synthesis and crystal structure of the mixed-cation borate Ga 4 In 4 B 15 O 33 (OH) 3