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The germanides Sr 3 Pd 4 Ge 4  and BaPdGe were obtained from high-temperature reactions in sealed niobium ampoules and their structures have been determined from single-crystal X-ray diffraction data:  a =444.2(1),  b =438.1(1),  c =2472.2(7) pm, space group  Immm , U 3 Ni 4 Si 4  type,  wR 2=0.0471, 576 unique reflections, 25 parameters for Sr 3 Pd 4 Ge 4  and  a =677.09(8), space group  P 2 1 3, LaIrSi type,  wR 2=0.0322, 409 unique reflections, nine parameters for BaPdGe. Both germanides have pronounced three-dimensional [Pd 4 Ge 4 ]  δ −  and [PdGe]  δ −  polyanionic networks with Pd–Ge bonding interactions. This is confirmed by the density functional theory (DFT)-based electronic structure investigations, the trends of charge transfer and crystal orbital overlap population (COOP) analyses.

The alkaline earth-palladium-germanides Sr 3 Pd 4 Ge 4 and BaPdGe