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A bisupporting Keggin-type polyoxometalate compound, {[Cu II (phen) 2 ] 2 [(HBW 12 O 40 )]}[Cu II Cl 2 (phen)] 2 · 2H 2 O (phen=1,10-phenathroline) ( 1 ), has been synthesized through the hydrothermal method and characterized by IR spectroscopy, elemental analysis, UV/Vis/NIR spectroscopy, and powder and single crystal X-ray diffraction. The bisupporting Keggin-polyoxometalate consists of one Keggin-type [HBW 12 O 40 ] 4−  core and two covalently linked copper(II) complex fragments [Cu(phen) 2 ] 2+ . In the crystal structure π···π interactions, C–H···Cl, O–H···Cl, O–H···O and C–H···O hydrogen bonds lead to a three-dimensional supramolecular structure.

Hydrothermal synthesis and crystal structure of a bisupporting Keggin-polyoxometalate hybrid compound decorated with a copper(II) complex unit