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Two transitional metal complexes, [Zn(oba)(3-bpcd)]  n   ( 1 ) and [Cd(oba)(3-bpcd) 0.5 ]  n   ( 2 ) [H 2 oba= 4,4′-oxybis(benzoic acid), 3-bpcd= N , N ′-bis(pyridin-3-yl)cyclohexane-1,4-dicarboxamide], have been hydrothermally synthesized and structurally characterized by elemental analyses, infrared spectra, powder X-ray diffraction, thermogravimetric and single-crystal X-ray diffraction. Complex  1  possesses a three-fold interpenetrating network based on layers with a 4-connected sql topology. Complex  2  is a layered framework constructed by the oba anions and 3-bpcd ligands, which represents a binodal (3,4)-connected {6 2 .10}{6} topology. The adjacent layers of complex  2  are further linked by hydrogen bonding interactions to build a three-dimensional supramolecular architecture. The differences of metal ions in coordination modes show a significant effect on the final structures of the Zn(II)/Cd(II) complexes. The photocatalytic activities and the fluorescence sensing properties of complexes  1  and  2  were investigated.

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Influence of different metal ions on the assembly, structures, and properties of two complexes based on the semi-rigid bis(pyridyl)-bis(amide) ligand and 4,4′-oxybis(benzoic acid)